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KMID : 1059520170610040151
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Journal of the Korean Chemical Society
2017 Volume.61 No. 4 p.151 ~ p.156
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A Simple, Efficient, Catalyst-Free and Solvent-Less Microwave-Assisted Process for N-Cbz Protection of Several Amines
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Aouf Zineb
Mansouri Rachida
Lakrout Salah
Berredjem Malika
Aouf Nour-Eddine
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Abstract
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A simple, green and chemo-selective method for the N-benzyloxycarbonylation of amines, β-amino alcohols, α- amino esters and sulfonamides has been developed under microwave irradiation. Good to excellent yields of the N-benzyloxycarbamates compounds were obtained in short times without any side products.
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KEYWORD
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Amine, Benzyl chloroformate (Cbz-Cl), Protection, Microwave-assisted, Solvent-free
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